中阶梯光栅厚铝膜硬度计算方法修正

Modified calculation method for thick aluminum film hardness of echelle grating

  • 摘要: 为了排除Pile-up现象对真空镀制机刻光栅厚铝膜在纳米压痕测试硬度中的影响, 获得中阶梯光栅铝膜准确硬度值, 提出通过修正O&P法中接触投影面积的新硬度计算方法。首先, 参照中阶梯光栅成槽深度, 采用连续刚度测试模式, 对中阶梯光栅厚铝膜进行压入深度为5 μm的纳米压痕硬度测试。其次, 对压痕位置进行SEM与AFM测试, 结果表明厚铝膜在纳米压痕硬度测试中出现Pile-up现象。最后, 对铝膜纳米压痕数据分析、提取, 压痕隆起形貌复原等, 证明接触面投影面积边缘为抛物线, 进而对O&P法中接触投影面积的计算方法进行修正。结果表明: 采用纳米压痕硬度测试方法, 中阶梯光栅厚铝膜的硬度值随着压深增加而增加, 采用修正接触投影面积的硬度修正计算方法获得的硬度值比传统O&P法所得硬度值减少40%左右。

     

    Abstract: In order to eliminate the impact of Pile-up phenomenon on the hardness of thick aluminum film of echelle grating in nano-indentation test, and obtain the accurate hardness value of aluminum film of echelle grating, a new hardness calculation method by modifying the contact projection area in O&P method was proposed.First of all, according to the groove depth of the echelle grating and adopting the CSM(continuous stiffness measurement), the nanoindentation hardness of the thick aluminum film of echelle grating with a pressing depth of 5 μm was tested.Secondly, SEM and AFM tests were carried out on the indentation position, and the results showed that pile-up phenomenon appeared in the nanoindentation hardness test of thick aluminum film.Finally, the analysis and extraction of nanoindentation data of aluminum film, and the recovery of indentation uplift morphology, etc. prove that the projected area edge of contact surface is a parabola, and then modify the calculation method of the projected area in O&P method.The results show that the hardness value of the thick aluminum film of the medium step grating increases with the increase of the pressing depth by the nano-indentation hardness test method, and the hardness value obtained by the modified contact projection area hardness correction method is about 40% lower than that obtained by the traditional O&P method

     

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